Optimization of Acid Pretreatment Assisted Degumming Process of Bamboo Sheath Fiber
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摘要: 以竹笋壳为研究对象,采用酸预处理结合碱氧-浴法脱胶工艺获取竹笋壳纤维,讨论脱胶工艺中氢氧化钠、过氧化氢用量及处理温度和时间对脱胶性能的影响。以残胶率为考查指标,通过正交实验得到碱氧-浴脱胶的最佳工艺参数为:氢氧化钠用量为24 g·L-1、过氧化氢用量为35 mL·L-1、煮练温度为95℃、碱煮时间为3 h,此时纤维残胶率为15.10%,并借助红外光谱分析仪测试提取的竹笋壳纤维的结构。所制备的竹笋壳纤维将被认为是一种有前途的、可持续发展的纺织工业原料,并具有广阔的应用前景。Abstract: The bamboo sheath fiber was obtained by acid pretreatment combined with alkali oxygen one bath degumming process. The effects of sodium hydroxide and hydrogen peroxide dosage,treatment temperature and time on degumming properties were explored. In terms of the percentage of residual gum, the optimum technological parameters were as follows:the dosage of sodium hydroxide was 24 g·L-1,the dosage of hydrogen peroxide was 35 mL·L-1,the treatment temperature was 95℃, and the alkali treatment time was 3 h. At this time,the fiber residue rate was 15.10%. The structure of the extracted bamboo sheath fiber was tested by infrared spectrum analyzer. The prepared bamboo sheath fiber will be considered as a promising and sustainable raw material for textile industry,and has broad application prospects.
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[1] Ye L Y,Zhang J M,Zhao J,et al. Properties of biochar obtained from pyrolysis of bamboo shoot shell[J].Journal of Analytical and Applied Pyrolysis,2015,114:172-178. [2] 孔令燕,曲丽君.不同植物纤维在纺织上的应用现状[J].中国麻业科学,2006,28(5):249-253. [3] Coseri S,Biliuta G,Simionescu B C,et al. Oxidized cellulose-survey of the most recent achievements[J]. Carbohydrate Polymers,2013,93:207-215. [4] Deng L,Geng M J,Zhu D W,et al. Effect of chemical and biological degumming on the adsorption of heavy metal by cellulose xan thogenates prepared from Eichhornia crassipes[J]. Bioresource Technology,2012,107:41-45. [5] Yang Y Z,Zhu M T,Fan F W,et al. Extaction of bamboo shoot shell fibers by the ultrasound assisted alkali oxygen bath method[J]. Cellulose chemistry and technology,2021(5-6):675-680. [6] Chen G,Bu F,Chen X,et al. Ultrasonic extraction,structural characterization,physicochemical properties and antioxidant activities of polysaccharides from bamboo shoots (Chimonobambusa quadrangularis) processing by-products[J]. International Journal of Biological Macromolecules,2018(112):656-666. [7] Pandiarajan P,Kathiresan M,Baskaran P G,et al. Characterization of raw and alkali treated new cellulosic fiber from the rinds of Thespesia populnea plant[J]. Journal of Natural Fibers,2020,1852996. [8] 朱梦婷,谢锦鹏,方凯炀,等.剑麻纤维脱胶处理的探究[J]. 武汉纺织大学学报,2021(4):49-52. [9] Soukaina Ajouguim,Karima Abdelouahdi,Mohamed Waqif,et al. Modifications of Alfa fibers by alkali and hydrothermal treatment[J]. Cellulose,2019(26):1503-1516. [10] Zhou J J,Li Z L,Yu C W. Property of ramie fiber degummed with Fenton reagent[J]. Fibers and Polymers,2017,18(10):1891-1897. [11] 周晓洁,李建强,陈延兴. 竹笋壳纤维脱胶方案的优化[J]. 上海纺织科技,2010,38(11):17-18,62. [12] Cui Y,Jia M L,Liu L,et al.Research on the character and degumming process of different parts of ramie fiber[J].Textile Research Journal,2017:1-11. [13] 孙颖,陈嘉琳,丁可欣,等. 乌拉草超声波预处理脱胶工艺[J]. 印染,2019,45(9):20-23. [14] Fan F W,Zhu M T,Fang K Y,et al. Comparitive study on enhanced pectinase and alkali-oxygen degummings of Sisal Fibers[J]. Cellulose,2021,28(13):8375-8386. [15] Ibrahim M M,Zawawy W K,Juttke Y,et al. Cellulose and microcrystalline cellulose from rice straw and banana plant waste:preparation and characterization[J]. Cellulose,2013,20(5):2403-2416. [16] 杜瑛,齐卫艳,苗霞,等.毛竹的主要化学成分分析及热解[J].化工学报,2004(12):2099-2102. [17] Gong W,Ran Z,Ye F,et al. Lignin from bamboo shoot shells as an activator and novel immobilizing support for α-amylase[J]. Food Chemistry,2017,228:455-462. [18] Łojewskaa J,Miskowieca P,Łojewskia T,et al. Cellulose oxidative and hydrolytic degradation:Insitu FTIR approach[J]. Polymer Degradation and Stability. 2005(88):512-520. [19] 倪海燕,付世伟,甘应进,等.竹笋壳纤维的微观结构与热性能测定[J].广西农业科学,2014,45(5):829-832. [20] Gopinath R,Billigraham P,Sathishkumar T P. Physicochemical and thermal properties of cellulosic fiber extracted from the bark of albizia saman[J]. Journal of Natural Fibers,2021,1929654.
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